3 A molecular sieve; oxygen; (-)-sparteine; dichloro bis(acetonitrile) palladium(II) in 1,2-dichloro-ethane T=70°C; 20 h; Title compound not separated from byproducts;
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Mandal, Sunil K.; Sigman, Matthew S.
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7535 - 7537
1: (PhO)2P(O)N3, DBU / toluene / Ambient temperature 2: H2 / PtO2 / ethanol / Ambient temperature View Scheme
参考文献
Wichmann, Juergen; Adam, Geo; Roever, Stephan; Cesura, Andrea M.; Dautzenberg, Frank M.; Jenck, Francois
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 16 p. 2343 - 2348
Wichmann, Juergen; Adam, Geo; Roever, Stephan; Cesura, Andrea M.; Dautzenberg, Frank M.; Jenck, Francois
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 16 p. 2343 - 2348