3,4-二氢-5,7,8-三甲基-1(2H)-萘酮合成路线 (共 5 条)
参考文献
Cocker et al.
Journal of the Chemical Society, 1953 , p. 2355,2359
反应条件
sulfuric acid
T=100°C; 2 h;
参考文献
Boberg, Friedrich; Jachiewicz, Adam; Garming, Alfons
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 72, # 1-4 p. 1 - 12
反应条件
1: N2H4+H2O; diethylene glycol / 100 °C / anschliessend Erhitzen mit KOH auf 250grad
2: aqueous H2SO4
View Scheme
参考文献
Cocker et al.
Journal of the Chemical Society, 1952 , p. 73,75
Journal of the Chemical Society, 1953 , p. 2355,2362
反应条件
1: AlCl3
2: N2H4*H2O, KOH / bis-(2-hydroxy-ethyl) ether / 250 °C
3: (i) SOCl2, (ii) AlCl3
View Scheme
参考文献
Buu-Hoi,N.P.; Saint-Ruf,G.
Journal of the Chemical Society, 1962 , p. 2630 - 2632
反应条件
1: amalgamated zinc; aqueous HCl
2: palladium/charcoal / 260 - 280 °C
View Scheme
参考文献
Cocker et al.
Journal of the Chemical Society, 1952 , p. 73,75
Journal of the Chemical Society, 1953 , p. 2355,2362