3-溴-5-硝基苯甲酸甲酯合成路线 （共 8 条）
反应条件
sulfuric acid; dibromoisocyanuric acid
参考文献
Khan, Anzar; Hecht, Stefan
Chemistry - A European Journal, 2006 , vol. 12, # 18 p. 4764 - 4774
反应条件
1: 5-Bromo-3-nitrobenzoic acid With oxalyl dichloride in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 1 h; 2: methanol in tetrahydrofuran; N,N-dimethyl-formamide T=0°C;
参考文献
Mori, Mattia; Vignaroli, Giulia; Cau, Ylenia; Dinic, Jelena; Hill, Richard; Rossi, Matteo; Colecchia, David; Pesic, Milica; Link, Wolfgang; Chiariello, Mario; Ottmann, Christian; Botta, Maurizio
ChemMedChem, 2014 , vol. 9, # 5 p. 973 - 983
反应条件
1: m-nitrobenzoic acid methyl ester With sulfuric acid; bromine; silver sulphate T=90°C; 1.5 h; 2: methanol With sulfuric acid Reflux;
参考文献
Kakuta, Hiroki; Azumaya, Isao; Masu, Hyuma; Matsumura, Mio; Yamaguchi, Kentaro; Kagechika, Hiroyuki; Tanatani, Aya
Tetrahedron, 2010 , vol. 66, # 42 p. 8254 - 8260
反应条件
sulfuric acid; bromine; silver sulphate T=90°C; 1.5 h;
参考文献
Tetrahedron, , vol. 66, # 42 p. 8254 - 8260
反应条件
1.1: sulfuric acid; N-bromosuccinmide / 12 h / 60 °C 2.1: oxalyl dichloride / tetrahydrofuran; N,N-dimethyl-formamide / 1 h / 20 °C 2.2: 0 °C View Scheme
参考文献
ChemMedChem, , vol. 9, # 5 p. 973 - 983
反应条件
1: With hydrogenchloride; iron in ethanol; water 5 h; Reflux; 2: With sodium carbonate in methanol; water
参考文献
Kakuta, Hiroki; Azumaya, Isao; Masu, Hyuma; Matsumura, Mio; Yamaguchi, Kentaro; Kagechika, Hiroyuki; Tanatani, Aya
Tetrahedron, 2010 , vol. 66, # 42 p. 8254 - 8260
参考文献
Mindl,J.; Vecera,M.
Collection of Czechoslovak Chemical Communications, 1973 , vol. 38, p. 3496 - 3505
反应条件
1.1: iron; hydrogenchloride / methanol; water / |Reflux 2.1: sulfuric acid / water / 0 °C / |Cooling with ice 2.2: 0.5 h / 0 °C / |Cooling with ice; |Reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 46 p. 17408 - 17416
