1-羟基-2-氧代-环己烷-1-羧酸乙酯合成路线 (共 7 条)
反应条件
iodine; sodium acetate in tetrahydrofuran; water
T=35°C; 2 h; IrradiationGreen chemistry;
参考文献
Miao, Chun-Bao; Wang, Yan-Hong; Xing, Meng-Lei; Lu, Xin-Wei; Sun, Xiao-Qiang; Yang, Hai-Tao
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11584 - 11589
反应条件
oxygen; Manganese (II) acetate in dichloromethane
T=23°C; Oxidation; P=760 Torr; 72 h;
参考文献
Christoffers, Jens
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7668 - 7669
反应条件
cerium(III) chloride; oxygen in isopropyl alcohol
T=23°C; 16 h;
参考文献
Christoffers, Jens; Werner, Thomas; Unger, Sven; Frey, Wolfgang
European Journal of Organic Chemistry, 2003 , # 3 p. 425 - 431
反应条件
di(n-butyl)tin oxide in toluene
18 h; Heating;
参考文献
Crout, David H. G.; Rathbone, Daniel L.
Journal of the Chemical Society, Chemical Communications, 1987 , # 4 p. 290 - 291
反应条件
oxygen; cerium(III) chloride in isopropyl alcohol
T=23°C; 16 h;
参考文献
Christoffers, Jens; Werner, Thomas; Frey, Wolfgang; Baro, Angelika
European Journal of Organic Chemistry, 2003 , # 24 p. 4879 - 4886
反应条件
water; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=50°C;
参考文献
Duschek, Alexander; Kirsch, Stefan F.
Chemistry - A European Journal, 2009 , vol. 15, # 41 p. 10713 - 10717
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=23°C; 6.5 h;
参考文献
Duschek, Alexander; Kirsch, Stefan F.
Chemistry - A European Journal, 2009 , vol. 15, # 41 p. 10713 - 10717