反应条件
1: 35.5 g / aq. KOH / methanol / 4 h / Heating
2: 1.) EtMgBr, 2.) CuCN, HMPT / 1.) THF, RT, 2 h, 2.) THF, 3 h
3: 79 percent / conc. H2SO4 / CCl4 / 10 h
4: LiAlH4 / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 20 h / 145 - 150 °C
5: 88 percent / pyridine / 24 h / Ambient temperature
View Scheme
参考文献
Gocan, Alexandra; Gansca, Lucia; Oprean, Ioan
Revue Roumaine de Chimie, 1995 , vol. 40, # 3 p. 253 - 258
