N-(叔丁氧基羰基)-L-亮氨酸甲酯合成路线 （共 29 条）
反应条件
in acetonitrile T=20°C;
参考文献
Sameiro, M; Goncalves, T; Maia, Hernani L.S
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7775 - 7777
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Sameiro; Goncalves; Maia, Hernani L.S.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 9 p. 1480 - 1485
反应条件
1: methanol; [14C]-L-(+)-Leucine With thionyl chloride Heating; 2: di-tert-butyl dicarbonate With sodium hydrogencarbonate in 1,4-dioxane; water T=20°C; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 73, # 13 p. 5180 - 5182
反应条件
triethylamine in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Sudhakar, Gangarajula; Bayya, Shruthi; Reddy, Karla Janardhan; Sridhar, Balasubramanian; Sharma, Komal; Bathula, Surendar Reddy
European Journal of Organic Chemistry, 2014 , vol. 2014, # 6 p. 1253 - 1265
反应条件
1: 99 percent / DMAP / acetonitrile / 20 °C 2: 49 percent / acetonitrile / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 9 p. 1480 - 1485
反应条件
1: 59 percent / DCC; HOBt / dimethylformamide 2: 99 percent / DMAP / acetonitrile 3: 49 percent / acetonitrile / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 44 p. 7775 - 7777
反应条件
potassium hydrogencarbonate in N,N-dimethyl-formamide 4 h; Ambient temperature;
参考文献
Bulletin of the Polish Academy of Sciences, Chemistry, , vol. 42, # 1 p. 117 - 130
反应条件
4-(N,N-dimethlyamino)pyridine; hydrazine 1.) THF, reflux, 6 h, 2.) MeOH, room temperature, 3 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 62, # 20 p. 7054 - 7057
反应条件
Bacillus licheniformis in water pH=7.8; Heating;
参考文献
Tetrahedron Asymmetry, , vol. 17, # 13 p. 1995 - 1999
反应条件
1: mercaptoacetic acid; triethylamine / 0.08 h / 20 °C / |Ionic liquid 2: 20 °C / |Ionic liquid View Scheme
参考文献
RSC Advances, , vol. 4, # 6 p. 2678 - 2686
