反应条件
1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 1.2: 0 - 20 °C 2.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 20 °C / Cooling with ice View Scheme
参考文献
Lin, Yih-Shyan; Park, Jaeok; De Schutter, Joris W.; Huang, Xian Fang; Berghuis, Albert M.; Sebag, Michael; Tsantrizos, Youla S.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 7 p. 3201 - 3215