2-(2-吡咯烷乙基)吡啶合成路线 （共 7 条）
反应条件
1,4-dioxane; nickel T=125°C; P=102971 Torr; Hydrogenation;
参考文献
Chough
Seoul Univ. J.Chem.Abstr., 1959 , vol. <C> 8, p. 335,349
Seoul Univ. J.Chem.Abstr., 1960 , p. 13129
反应条件
1: 54 percent Chromat. / PPh3 / [Rh(cod)2]BF4 / tetrahydrofuran / 20 h / Heating
2: 21 percent Chromat. / Pd/C / tetrahydrofuran / 48 h / 760 Torr
View Scheme
参考文献
Beller, Matthias; Trauthwein, Harald; Eichberger, Martin; Breindl, Claudia; Mueller, Thomas E.
European Journal of Inorganic Chemistry, 1999 , # 7 p. 1121 - 1132
反应条件
methanol; acetic acid
参考文献
Reich; Levine
Journal of the American Chemical Society, 1955 , vol. 77, p. 4913
反应条件
triphenylphosphine; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate in tetrahydrofuran
Alkylation; 20 h; Heating;
参考文献
Beller, Matthias; Trauthwein, Harald; Eichberger, Martin; Breindl, Claudia; Mueller, Thomas E.
European Journal of Inorganic Chemistry, 1999 , # 7 p. 1121 - 1132
反应条件
in acetonitrile
T=20°C;
参考文献
Nersesian, Diana L.; Black, Lawrence A.; Miller, Thomas R.; Vortherms, Timothy A.; Esbenshade, Timothy A.; Hancock, Arthur A.; Cowart, Marlon D.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 1 p. 355 - 359
反应条件
1: water; formic acid; hydrogen / 240 °C / 103707 Torr
2: KOH / unter Ausschluss von Licht und anschl. Erwaermen unter 12 Torr
3: acetic acid / 150 °C
View Scheme
参考文献
Profft
CHEMTECH, 1955 , vol. 7, p. 511,517
反应条件
1: KOH / unter Ausschluss von Licht und anschl. Erwaermen unter 12 Torr
2: acetic acid / 150 °C
View Scheme
参考文献
Profft
CHEMTECH, 1955 , vol. 7, p. 511,517
