(4-甲氧基苯基)-萘-1-胺合成路线 （共 11 条）
反应条件
1: 4-methoxy-aniline With C40H50BrCl2N3Pd; potassium tert-butylate
T=20°C; Schlenk techniqueInert atmosphere;
2: alpha-chloronaphthalene in toluene
T=100°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Fang, Weiwei; Jiang, Jian; Xu, Yong; Zhou, Juefei; Tu, Tao
Tetrahedron, 2013 , vol. 69, # 2 p. 673 - 679
反应条件
sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate in xylene
21 h; Inert atmosphereReflux;
参考文献
Sony Corporation
Patent: US8063200 B2, 2011 ;
Location in patent: Page/Page column 19-20 ;
反应条件
sodium t-butanolate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; chlorobis(triphenylphosphine)(1-naphthyl)nickel(II) in 1,4-dioxane
T=110°C; 0.5 h;
参考文献
Gao, Cai-Yan; Yang, Lian-Ming
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1624 - 1627
反应条件
cBRIDP; bis(η3-allyl-μ-chloropalladium(II)); NaO-t-am in water
T=20°C; 1.5 h; Inert atmosphereMicellar solution;
参考文献
Lipshutz, Bruce H.; Chung, David W.; Rich, Brian
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1717 - 1721
反应条件
tetrabutylammomium bromide; oxygen; palladium diacetate in dimethyl sulfoxide
T=60°C; P=760.051 Torr; 12 h;
参考文献
Wei, Ye; Deb, Indubhusan; Yoshikai, Naohiko
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9098 - 9101
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
T=120°C;
参考文献
Shan, Jingning; Yap, Glenn P. A.; Richeson, Darrin S.
Canadian Journal of Chemistry, 2005 , vol. 83, # 6-7 p. 958 - 968
反应条件
water; sodium hydrogensulfite
T=120°C;
参考文献
I.G.Farbenind.
Patent: DE530825 , 1926 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 604
参考文献
Knoll and Co.
Patent: DE241853 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 180
Full Text Show Details
Knoevenagel
Journal fuer Praktische Chemie (Leipzig), 1914 , vol. <2>89, p. 45
参考文献
Bayer and Co.
Patent: DE80669 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 136
反应条件
1: iodine; sulfur
2: NaNH2; toluene / anschliessend Behandeln mit Diaethyl-<2-chlor-aethyl>-amin
View Scheme
参考文献
Talukdar; Shirley
Journal of the American Chemical Society, 1958 , vol. 80, p. 3462,3464, 3466
