(2,2-二乙氧基乙基)-苯合成路线 (共 26 条)
反应条件
1: 66 percent / formic acid / 24 h
2: 50 percent / tetrahydrofuran / 12 h / 20 °C
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参考文献
Beaudet, Isabelle; Duchene, Alain; Parrain, Jean-Luc; Quintard, Jean-Paul
Journal of Organometallic Chemistry, 1992 , vol. 427, # 2 p. 201 - 212
反应条件
anschliessendes Kochen;
参考文献
Blicke; Kaplan
Journal of the American Chemical Society, 1943 , vol. 65, p. 1967,1968
反应条件
n-butyllithium in tetrahydrofuran; hexane
1.) -78 deg C; 2.) up to 0 deg C; Yield given. Yields of byproduct given;
参考文献
Parrain, Jean-Luc; Beaudet, Isabelle; Cintrat, Jean-Christophe; Duchene, Alain; Quintard, Jean-Paul
Bulletin de la Societe Chimique de France, 1994 , vol. 131, # 3 p. 304 - 312
反应条件
AuCl3-CuCl2
4 h; Heating;
参考文献
Zhang, Xin; Corma, Avelino
Chemical Communications, 2007 , # 29 p. 3080 - 3082
反应条件
n-butyllithium
1.) THF, -78 deg C, 2.) THF; Yield given. Multistep reaction;
参考文献
Quintard, Jean-Paul; Elissondo, Bernard; Pereyre, Michel
Journal of Organometallic Chemistry, 1981 , vol. 212, # 3 p. C31 - C34
参考文献
Dufraisse; Chaux
Bulletin de la Societe Chimique de France, 1926 , vol. <4> 39, p. 905,912, 914
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Wood; Comley
Journal of the Society of Chemical Industry, London, 1923 , vol. 42, p. 342 T
Chem. Zentralbl., 1924 , vol. 95, # I p. 418
参考文献
Sigmund
Monatshefte fuer Chemie, 1928 , vol. 49, p. 279
参考文献
Tomioka, Hideo; Hayashi, Norihiro; Izawa, Yasuji; Liu, Michael T. H.
Tetrahedron Letters, 1984 , vol. 25, # 39 p. 4413 - 4416
反应条件
in benzene
T=10.1°C; Irradiationactivation energie, ΔS(act.); Thermodynamic dataKineticsRate constant;
参考文献
Liu, Michael T. H.; Subramanian, Ramasamy
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1233 - 1240
反应条件
trifluoroacetic acid
T=60°C; 50 h; effect of additives; rate const. at 60 deg C; Product distributionRate constantMechanism;
参考文献
Okuyama, Tadashi; Ishida, Yoshimi; Ochiai, Masahito
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 2 p. 163 - 170