7H-苯并[c]氧杂蒽-7-酮合成路线 (共 19 条)
反应条件
tetra-n-butylammonium difluorotriphenylsilicate(IV) in toluene
T=60°C; 24 h;
参考文献
Dubrovskiy, Anton V.; Larock, Richard C.
Tetrahedron, 2013 , vol. 69, # 13 p. 2789 - 2798
反应条件
potassium phosphate in toluene
T=110°C; 2 h; Inert atmosphereSchlenk techniqueGreen chemistry;
参考文献
Menendez, Cintia A.; Nador, Fabiana; Radivoy, Gabriel; Gerbino, Dario C.
Organic Letters, 2014 , vol. 16, # 11 p. 2846 - 2849
反应条件
cesium fluoride in tetrahydrofuran
T=65°C; 24 h;
参考文献
Zhao, Jian; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 19 p. 4273 - 4275
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Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588
反应条件
sodium t-butanolate in water
T=20 - 100°C; regioselective reaction;
参考文献
Barbero, Nekane; SanMartin, Raul; Dominguez, Esther
Tetrahedron, 2009 , vol. 65, # 29-30 p. 5729 - 5732
反应条件
sodium t-butanolate in water
T=20 - 100°C;
参考文献
Barbero, Nekane; SanMartin, Raul; Dominguez, Esther
Tetrahedron, 2009 , vol. 65, # 29-30 p. 5729 - 5732
反应条件
tert.-butylhydroperoxide; Rhodium trichloride; triphenylphosphine in chlorobenzene
T=160°C; 24 h; Inert atmosphere;
参考文献
Wang, Ping; Rao, Honghua; Hua, Ruimao; Li, Chao-Jun
Organic Letters, 2012 , vol. 14, # 3 p. 902 - 905
反应条件
copper(l) iodide; N,N,N',N,-tetramethylethylenediamine in water
T=120°C; 15 h;
参考文献
Barbero, Nekane; Sanmartin, Raul; Dominguez, Esther
Green Chemistry, 2009 , vol. 11, # 6 p. 830 - 836
反应条件
palladium diacetate; CsO2CCMe3 in water; N,N-dimethyl-formamide
T=130°C; 3 h; Reagent/catalystTemperatureTimeSolvent; regioselective reaction;
参考文献
Cheng, Ming; Yan, Jianwei; Hu, Feng; Chen, Hong; Hu, Youhong
Chemical Science, 2013 , vol. 4, # 1 p. 526 - 530
反应条件
oxygen; rose bengal in acetonitrile
64 h; Irradiation;
参考文献
Xu, Wen-Zhi; Huang, Zhi-Tang; Zheng, Qi-Yu
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5606 - 5608
反应条件
trifluorormethanesulfonic acid; silica gel; ytterbium(III) triflate
Friedel Crafts reaction; 0.0833333 h; Neat (no solvent)Microwave irradiation;
参考文献
Li, Jie; Jin, Can; Su, Weike
Heterocycles, 2011 , vol. 83, # 4 p. 855 - 866