2-癸基-1,3-二氧戊环合成路线 （共 5 条）
反应条件
sulfuric acid 10 h; Ambient temperature;
参考文献
Iwamoto, Minoru; Kubota, Noboru; Takagi, Yoshikazu; Kogami, Kunio; Hayashi, Kazuo
Agricultural and Biological Chemistry, 1982 , vol. 46, # 9 p. 2383 - 2386
参考文献
EVONIK DEGUSSA GmbH
Patent: US2012/22276 A1, 2012 ;
Location in patent: Page/Page column 6-7 ;
反应条件
sodium hydrogen sulphate; silica gel
Etherification; Acetalization; 0.0833333 h; microwave irradiation;
参考文献
Yadav; Reddy, B. V. Subba; Srinivas; Ramalingam
Synlett, 2000 , # 5 p. 701 - 703
反应条件
1: 92 percent / NaI, 18-crown-6 / toluene; dimethylsulfoxide / 6 h / 90 - 100 °C
2: 1.) Mg, 2.) Li2CuCl4 / 1.) THF, 2.) r.t., 1 h
View Scheme
参考文献
Iwamoto, Minoru; Kubota, Noboru; Takagi, Yoshikazu; Kogami, Kunio; Hayashi, Kazuo
Agricultural and Biological Chemistry, 1982 , vol. 46, # 9 p. 2383 - 2386
反应条件
dilithium tetrachlorocuprate; magnesium
1.) THF, 2.) r.t., 1 h; Yield given. Multistep reaction;
参考文献
Iwamoto, Minoru; Kubota, Noboru; Takagi, Yoshikazu; Kogami, Kunio; Hayashi, Kazuo
Agricultural and Biological Chemistry, 1982 , vol. 46, # 9 p. 2383 - 2386
