air in pentane T=0°C; Kinetics; Further Variations:TemperaturesSolventsReagents;

HgCl2 or HCl in ethanol refluxing soln. of educts with stirring, react. in presence of HgCl2 or dry HCl gas under N2; cooling, pptn., filtration, washing (EtOH, water, EtOH, ether), drying in vacuo, fractional crystn. (CH2Cl2-C6H6), recrystn. from light petroleum ether, (dicarbonyl complex recrystd. from CH2Cl2-MeOH);

1: With isopentyl nitrite in dichloromethane T=20°C; Darkness; 2: With methanol in dichloromethane T=-25°C; 2 h; Darkness;

in acetonitrile T=25°C; Equilibrium constant;

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