4-(3-羟基-1-丙炔)苯甲酸合成路线 (共 3 条)
反应条件
triethylamine; triphenylphosphine; copper(l) iodide; Pd(TPPMS)2Cl2 in water
T=25°C; 1 h; other aryl iodides;
参考文献
Bumagin, N. A.; Bykov, V. V.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 3 p. 348 - 350
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 3 p. 385 - 387
反应条件
1: PEG 4000 bound 4-iodobenzoic acid With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate
0.025 h; microwave irradiation;
2: propargyl alcohol With sodium hydroxide
0.0333333 h; microwave irradiation;
参考文献
Xia, Min; Wang, Yan-Guang
Journal of Chemical Research - Part S, 2002 , # 4 p. 173 - 175
反应条件
morpholine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in dichloromethane; water
Sonogashira coupling;
参考文献
Tulla-Puche, Judit; Barany, George
Tetrahedron, 2005 , vol. 61, # 8 p. 2195 - 2201