反应条件
1: 79 percent / tin(IV) chloride / benzene / 2 h / -5 - 20 °C
2: 85 percent / hydroxylamine hydrochloride; barium carbonate / ethanol / 8 h / Heating
3: 32 percent / PCl5 / diethyl ether / 0.75 h / 0 - 20 °C
4: 82 percent / tin(IV) chloride / 1,2-dichloro-ethane / 10.5 h / Heating
5: 98 percent / aq. KOH / methanol / 0.75 h / Heating
View Scheme
参考文献
Tranberg, C. Elisabet; Zickgraf, Andrea; Giunta, Brian N.; Luetjens, Henning; Figler, Heidi; Murphree, Lauren J.; Falke, Ruediger; Fleischer, Holger; Linden, Joel; Scammells, Peter J.; Olsson, Ray A.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 2 p. 382 - 389
