1,1,2,2-四苯基乙烷合成路线 （共 396 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate
T=155 - 160°C; 0.166667 h;
参考文献
Khurana, Jitender M.; Chauhan, Sushma; Maikap, Golak C.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 10 p. 1737 - 1740
反应条件
1: 60 percent / 1) KOH / 1) methanol, 2) neat, 150 deg C, 2 h
2: acetonitrile / 2 h / Irradiation
3: acetonitrile / 14 h / Irradiation
View Scheme
参考文献
Freccero, Mauro; Fasani, Elisa; Albini, Angelo
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1740 - 1745
反应条件
1: 2) 25 percent aq. ammonia / 1) neat, 135 - 140 deg C, 6 h, 2) 12 h
2: 20 percent / thionyl chloride / dimethylformamide / 7 h / 60 - 70 °C
3: 60 percent / 1) KOH / 1) methanol, 2) neat, 150 deg C, 2 h
4: acetonitrile / 2 h / Irradiation
5: acetonitrile / 14 h / Irradiation
View Scheme
参考文献
Freccero, Mauro; Fasani, Elisa; Albini, Angelo
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1740 - 1745
反应条件
1: 20 percent / thionyl chloride / dimethylformamide / 7 h / 60 - 70 °C
2: 60 percent / 1) KOH / 1) methanol, 2) neat, 150 deg C, 2 h
3: acetonitrile / 2 h / Irradiation
4: acetonitrile / 14 h / Irradiation
View Scheme
参考文献
Freccero, Mauro; Fasani, Elisa; Albini, Angelo
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1740 - 1745
反应条件
aluminium trichloride; benzene
参考文献
Fleck; Preston; Haller
Journal of the American Chemical Society, 1945 , vol. 67, p. 1419,1420
参考文献
Cohen; Wang
Journal of the American Chemical Society, 1955 , vol. 77, p. 2628,2631
反应条件
lithium aluminium tetrahydride; anhydrous butyl ether; benzene
参考文献
Cohen; Wang
Journal of the American Chemical Society, 1955 , vol. 77, p. 3628,3631
反应条件
diethyl ether; magnesium
Behandeln des Reaktionsgemisches mit Kohlendioxid bei -15grad;
参考文献
Gilman; Zoellner
Journal of the American Chemical Society, 1930 , vol. 52, p. 3984,3986
反应条件
benzene
Irradiation.Sonnenlicht;
参考文献
Mustafa et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 4306,4307
反应条件
hydrogenchloride; aluminium trichloride
参考文献
Alexander; Fuson
Journal of the American Chemical Society, 1936 , vol. 58, p. 1745
