1,1,2,2-四苯基乙烷合成路线 (共 396 条)
反应条件
hydrogenchloride; amalgamated zinc in water; toluene
24 h; Heating; Further byproducts given;
参考文献
Talapatra, Sunil K.; Chakrabarti, Syamal; Mallik, Asok K.; Talapatra, Bani
Tetrahedron, 1990 , vol. 46, # 17 p. 6047 - 6052
反应条件
di-tert-butyl peroxide
参考文献
Mignani, S.; Merenyi, R.; Janousek, Z.; Viehe, H. G.
Bulletin des Societes Chimiques Belges, 1984 , vol. 93, # 11 p. 991 - 998
参考文献
Benati, Luisa; Montevecchi, Pier Carlo; Spagnolo, Piero; Tundo, Antonio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1544 - 1548
反应条件
1: 74 percent
2: 7 percent Spectr. / AlCl3 / 0.08 h / other substrates
View Scheme
参考文献
Mall; Buchholz; Stamm
Archiv der Pharmazie, 1994 , vol. 327, # 6 p. 377 - 380
反应条件
2: 84 percent / p-toluenesulfonic acid / toluene / 0.17 h / Heating
3: acetic acid / methanol; various solvent(s) / 9 h / Irradiation
View Scheme
参考文献
Adam, Waldemar; Berkessel, Albrecht; Peters, Eva-Maria; Peters, Karl; Schnering, Hans Georg von
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2811 - 2814
反应条件
1: 84 percent / p-toluenesulfonic acid / toluene / 0.17 h / Heating
2: acetic acid / methanol; various solvent(s) / 9 h / Irradiation
View Scheme
参考文献
Adam, Waldemar; Berkessel, Albrecht; Peters, Eva-Maria; Peters, Karl; Schnering, Hans Georg von
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2811 - 2814
反应条件
in acetonitrile
Ar atmosphere, room temp.; stirring of Cu-compd. in MeCN (10 min), addn. of soln. of org. compd. in MeCN, stirring (1 h); removal of MeCN (vac.), extn. of org. compds.;
参考文献
Jacobson, Richard R.; Tyeklar, Zoltan; Karlin, Kennth D.
Inorganica Chimica Acta, 1991 , vol. 181, p. 111 - 118
反应条件
lithium aluminium tetrahydride; titanium(III) chloride; ammonia in tetrahydrofuran
T=67°C; Further byproducts given;
参考文献
Volckaerts, E.; Geise, H. J.; Daelmans, F.
Bulletin des Societes Chimiques Belges, 1992 , vol. 101, # 6 p. 503 - 508
反应条件
in acetonitrile
T=17°C; Irradiationalso with others benzylic donors; MechanismQuantum yield;
参考文献
Sulpizio, Ada; Albini, Angelo; d'Alessandro, Nicola; Fasani, Elisa; Pietra, Silvio
Journal of the American Chemical Society, 1989 , vol. 111, # 15 p. 5773 - 5777
反应条件
potassium hydroxide in methanol; acetonitrile
5 h; Irradiation;
参考文献
Fasani, E.; d'Alessandro, N.; Albini, A.; Mariano, P. S.
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 829 - 835