1,1,2,2-四苯基乙烷合成路线 (共 396 条)
反应条件
hydrogenchloride; acetic acid; zinc
2 h; Heating;
参考文献
Vona, Maria Luisa Di; Rosnati, Vittorio
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4269 - 4273
反应条件
magnesium
T=600°C; P=0.01 - 0.1 Torr;
参考文献
Aitken, R. Alan; Hodgson, Philip K.G.; Morrison, John J.; Oyewale, Adebayo O.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 402 - 415
反应条件
benzhydryllithium in tetrahydrofuran; hexane
12 h; Ambient temperature;
参考文献
Eisch, John J.; Tsai, Miin-Rong
Journal of Organometallic Chemistry, 1982 , vol. 225, # 1 p. 5 - 24
反应条件
ytterbium; methyl iodide in N,N,N',N',N'',N''-hexamethylphosphoric triamide; benzene
20 h; Ambient temperature;
参考文献
Makioka, Yoshikazu; Uebori, Shin-Ya; Tsuno, Masumi; Taniguchi, Yuki; Takaki, Ken; Fujiwara, Yuzo
Journal of Organic Chemistry, 1996 , vol. 61, # 1 p. 372 - 375
反应条件
1: acetonitrile / 15 h / Irradiation
2: acetonitrile / 14 h / Irradiation
View Scheme
参考文献
Freccero, Mauro; Fasani, Elisa; Albini, Angelo
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1740 - 1745
反应条件
1: acetonitrile / 40 h / Irradiation
2: acetonitrile / 14 h / Irradiation
View Scheme
参考文献
Freccero, Mauro; Fasani, Elisa; Albini, Angelo
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1740 - 1745
反应条件
1: 91.5 percent / triphenylmethyl tetrafluoroborate / acetonitrile / 0.5 h / Ambient temperature
2: LiCl / tetrahydrofuran / 1.) -60 deg C, 4 h; 2.) -60 -> 0 deg C, 2 h
View Scheme
参考文献
Komatsu, Koichi; Moriyama, Takamasa; Nishiyama, Tomihiro; Okamoto, Kunio
Tetrahedron, 1981 , vol. 37, p. 721 - 729
反应条件
n-butyllithium; Petroleum ether
参考文献
Wittig; Stahnecker
Justus Liebigs Annalen der Chemie, 1957 , vol. 605, p. 69,85
反应条件
in benzene
T=17°C; Irradiationwith Helios quartz light; Further byproducts given;
参考文献
Albini, Angelo; Fasani, Elisa; Frattini, Valeria
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 235 - 240
反应条件
in benzene
T=17°C; Irradiationwith Helios quartz light; Further byproducts given;
参考文献
Albini, Angelo; Fasani, Elisa; Frattini, Valeria
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 235 - 240