1,1,2,2-四苯基乙烷合成路线 (共 396 条)
反应条件
in benzene
T=120°C; 26 h; Further byproducts given;
参考文献
Mizuno, Hajime; Matsuda, Minoru; Iino, Masashi
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 520 - 525
反应条件
in benzene
T=120°C; 26 h; Further byproducts given;
参考文献
Mizuno, Hajime; Matsuda, Minoru; Iino, Masashi
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 520 - 525
反应条件
in cyclohexane
T=25°C; Irradiation;
参考文献
Savino, T. G.; Senthilnathan, V. P.; Platz, M. S.
Tetrahedron, 1986 , vol. 42, # 8 p. 2167 - 2180
反应条件
aluminium trichloride
0.0833333 h;
参考文献
Mall; Buchholz; Stamm
Archiv der Pharmazie, 1994 , vol. 327, # 6 p. 377 - 380
反应条件
[Co(triphenylphosphane)2Cl2]; potassium carbonate in chloroform
12 h; Heating; Yields of byproduct given;
参考文献
Noelke, Margot; Verevkin, Sergej P.; Beckhaus, Hans-Dieter; Ruechardt, Christoph
Liebigs Annalen, 1995 , # 1 p. 41 - 52
反应条件
1,4-diaza-bicyclo[2.2.2]octane in acetonitrile
0.05 h; Irradiation;
参考文献
Homma; Yamada
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 7 p. 1198 - 1201
反应条件
in acetonitrile
Photolysis;
参考文献
Koshima, Hideko
Molecular Crystals and Liquid Crystals, 2005 , vol. 440, p. 207 - 214
反应条件
CH3MgCl in diethyl ether; benzene
Norbornadiene-compound and Ph2CHCl are heated at 75°C for 4 h in benzene under Ar, methylation of Ph2CHCHPh2 and Ph2CHGeMe2Cl with MeMgCl in Et2O (stirring at 0°C for 0.5 h, followed by stirring for 1 h at room temp.).; addn. of H2O and NH4Cl, sepn. of organic and aq. phases, extn. of aq. phase (Et2O), removal of solvent, identification by GC-MS anal., further products are Me8Ge3, Me10Ge4, Me12Ge5 (yield: ca 5 percent);
参考文献
Koecher, Juergen; Lehnig, Manfred; Neumann, Wilhelm P.
Organometallics, 1988 , vol. 7, p. 1201 - 1207
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=20°C; 3 h; IrradiationInert atmosphereGreen chemistry; Quantum yield;
参考文献
Oksdath-Mansilla, Gabriela; Argueello, Juan E.; Penenory, Alicia B.
Tetrahedron Letters, 2013 , vol. 54, # 12 p. 1515 - 1518
反应条件
phosphorus; hydrogen iodide
T=170°C;
参考文献
Graebe
Chemische Berichte, 1875 , vol. 8, p. 1055