1,1,2,2-四苯基乙烷合成路线 (共 396 条)
反应条件
tetrahydrofuran; lithium
anschliessend Behandeln mit Methanol;
参考文献
Wittig; Schloer
Suomen Kemistilehti B, 1958 , vol. 31, p. 2,7
参考文献
Klinger; Lonnes
Chemische Berichte, 1896 , vol. 29, p. 2159
反应条件
diethyl ether; mercury dichloride
参考文献
Ziegler
Chemische Berichte, 1931 , vol. 64, p. 445,448
反应条件
aluminium trichloride
参考文献
Anschuetz
Justus Liebigs Annalen der Chemie, 1886 , vol. 235, p. 163
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Wang, Hanqing; Kispert, Lowell. D.; Sang, Hong
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1463 - 1470
反应条件
aluminium; mercury dichloride
Erhitzen zum Sieden; Behandeln mit α.β-Dichlor-aethylen oder Trichloraethylen;
参考文献
Boeeseken; Bastet
Recueil des Travaux Chimiques des Pays-Bas, 1913 , vol. 32, p. 189
反应条件
acetic acid in various solvent(s)
9 h; Irradiation;
参考文献
Adam, Waldemar; Berkessel, Albrecht; Peters, Eva-Maria; Peters, Karl; Schnering, Hans Georg von
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2811 - 2814
反应条件
18-crown-6 ether; potassium tert-butylate
1.) HMPA, 2.) irradiation, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russell, Glen A.; Khanna, Rajive K.
Tetrahedron, 1985 , vol. 41, # 19 p. 4133 - 4146
反应条件
p-toluenesulfinyl chloride; n-butyllithium
1.) n-hexane, THF, r.t., 1 h, 2.) n-hexane, THF, Et2O, r.t., 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Furukawa, Mitsuru; Okawara, Tadashi; Noguchi, Yoshihide; Nishikawa, Masumi; Tomimatsu, Masahide
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 976 - 978
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine
1.) hexane, 18h, room temperature, 2.) diethyl ether, pentane, 15 min, room temperature;
参考文献
Maercker, Adalbert; Berkulin, Willi
Chemische Berichte, 1990 , vol. 123, # 1 p. 185 - 192
反应条件
aluminum oxide; titanium(III) chloride in tetrahydrofuran
24 h; Heatingother reag.; other reaction time; Product distribution;
参考文献
Furstner; Seidel
Synthesis, 1995 , # 1 p. 63 - 68