1,1,2,2-乙烷四甲酸四乙酯合成路线 （共 104 条）
参考文献
Komnenos
Monatshefte fuer Chemie, 1910 , vol. 31, p. 119
反应条件
in methanol T=0°C; electrolysis, iron cathode, Pt anode, NaI electrolyte, 220 mA/cm2, 2.2 F/mol;
参考文献
Elinson, M. N.; Fedukovich, S. K.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 86 - 90
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 96 - 100
反应条件
1: 67 percent Turnov. / 50 °C / electrolysis, iron cathode, Pt anode, NaI electrolyte, 220 mA/cm2, 3.6 F/mol 2: 75 percent View Scheme
参考文献
Elinson, M. N.; Fedukovich, S. K.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 86 - 90
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 96 - 100
反应条件
T=50°C; electrolysis, iron cathode, Pt anode, NaI electrolyte, 220 mA/cm2, 3.6 F/mol;
参考文献
Elinson, M. N.; Fedukovich, S. K.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 86 - 90
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 96 - 100
反应条件
sodium ethanolate in ethanol
20 h; Heating;
参考文献
Jamrozik, Janusz
Monatshefte fuer Chemie, 1980 , vol. 111, p. 643 - 648
反应条件
1: tetraethyl ethane-1,1,2,2-tetracarboxylate With sodium hydride in tetrahydrofuran
T=20°C; 1 h;
2: 1-bromo-pent-2-yne in tetrahydrofuran
44 h; Heating;
参考文献
Tekavec, Thomas N.; Louie, Janis
Journal of Organic Chemistry, 2008 , vol. 73, # 7 p. 2641 - 2648
反应条件
1: lithium alanate; diethyl ether
2: acetic acid
3: 480 °C
View Scheme
参考文献
Bailey,W.J. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1724 - 1725
反应条件
(i) LiAlH4, Et2O, (ii) /BRN= 385737/; Multistep reaction;
参考文献
Bailey,W.J. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1724 - 1725
参考文献
Conrad; Bischoff
Justus Liebigs Annalen der Chemie, 1882 , vol. 214, p. 68
参考文献
Conrad; Bischoff
Justus Liebigs Annalen der Chemie, 1882 , vol. 214, p. 68
