1,1,2,2-乙烷四甲酸四乙酯合成路线 （共 104 条）
反应条件
1: 1.) sodium ethoxide / 1.) ethanol, reflux, 30 min, 2.) a.) 25 deg C, 30 min, b.) 60 deg C, 7 h
2: 1.) sodium hydride / 1.) THF, 25 deg C, 1 h, 2.) a.) 1 h, b.) reflux, 36 h
View Scheme
参考文献
Luk'yanenko, N. G.; Mel'nik, O. T.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 10.2 p. 1975 - 1983
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 10 p. 2186 - 2195
反应条件
potassium hydroxide in ethanol
0.5 h; Heating;
参考文献
Gao, Ying; Foersterling, Horst-Dieter; Noszticzius, Zoltan; Meyer, Bernhard
Journal of Physical Chemistry, 1994 , vol. 98, # 34 p. 8377 - 8380
反应条件
1: Na / ethanol / 2 h / 55 °C
2: conc HCl / 3 h / Heating
View Scheme
参考文献
Peng, Hairuo; Kim, Doeg-Il; Sarkaria, Jann N; Cho, Yong-Seo; Abraham, Robert T; Zalkow, Leon H
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 167 - 174
参考文献
Koetz; Stahlmann
Journal fuer Praktische Chemie (Leipzig), 1903 , vol. <2>68, p. 163
