6-氯-2,4-甲氧基嘧啶合成路线 (共 13 条)
反应条件
in methanol T=0 - 20°C; 3.5 h;
参考文献
Guo, Hongyan; Kim, Choung U.; Kim, Hae Soo; Lee, Chong-Kyo; Lee, Ill Young; Mitchell, Michael L.; Son, Jong Chan; Xu, Lianhong
Patent: US2008/70920 A1, 2008 ;
Location in patent: Page/Page column 99-100 ;
反应条件
phosphorus pentachloride; trichlorophosphate
参考文献
Journal of the American Chemical Society, , vol. 76, p. 6052
反应条件
in methanol T=20°C; Substitution;
参考文献
Pesticide Science, , vol. 47, # 2 p. 103 - 114
参考文献
Chemische Berichte, , vol. 36, p. 2234
参考文献
Bredereck et al.
Chemische Berichte, 1959 , vol. 92, p. 583,594
反应条件
sodium hydroxide; diethyl ether; palladium Hydrogenation;
参考文献
Smith; Christensen
Journal of Organic Chemistry, 1955 , vol. 20, p. 829,833,835
参考文献
Iwata, Masaki; Bruice, Thomas C.; Carrell, H. L.; Glusker, Jenny P,
Journal of the American Chemical Society, 1980 , vol. 102, # 15 p. 5036 - 5044
参考文献
Bergmann; Heimhold
Journal of the Chemical Society, 1935 , p. 955
Full Text Show Details
Fisher; Johnson
Journal of the American Chemical Society, 1932 , vol. 54, p. 727,731
反应条件
1: 90 percent / NaNO3, H2SO4 / 5 h / 80 °C
2: 95 percent / NH4OAc / tetrahydrofuran / 5 h / Heating
View Scheme
参考文献
Choy, Nakyen; Russell, Keith C.
Heterocycles, 1999 , vol. 51, # 1 p. 13 - 16
反应条件
in benzene
1) 0 deg C; 2) room temperature, 12h;
参考文献
Hermann, Klaus; Simchen, Gerhard
Liebigs Annalen der Chemie, 1981 , # 2 p. 333 - 341