反应条件
1.1: triethylamine / dichloromethane / 16 h / 20 °C 2.1: triethylamine; triphenylphosphine; 1,2,2-trichloro-1,1,2-trichloro-ethane / dichloromethane / 64 h / 20 °C 3.1: N,N-dimethyl-formamide / 16 h 4.1: sodium tetrahydroborate / methanol / 18 h / 0 - 20 °C 4.2: 0.08 h View Scheme
参考文献
ABBOTT HEALTHCARE PRODUCTS B.V.; SMID, Pieter; IWEMA BAKKER, Wouter, I.; COOLEN, Hein, K.A.C.; SLIEDREGT, Leonardus, A.J.M.; VAN DONGEN, Maria, J.P.; DEN HARTOG, Jacobus, A.J.
Patent: WO2012/4373 A1, 2012 ;
WO 2012/004373 A1