3-羟基-3,5-二甲基-己烷-2-酮合成路线 (共 6 条)
反应条件
sulfuric acid; mercuric sulphate
参考文献
Hennion; Watson
Journal of Organic Chemistry, 1958 , vol. 23, p. 656
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Papa et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 4441,4445
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Bergmann; Herman
Journal of Applied Chemistry, 1953 , vol. 3, p. 42,48
反应条件
[Co(η5-C5H5)2]; triethylamine
T=80°C; P=36775.4 Torr; 5 h;
参考文献
Inoue, Yoshio; Ishikawa, Jiro; Taniguchi, Masaaki; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 3 p. 1204 - 1206
反应条件
water; 2.) acid
Multistep reaction;
参考文献
Balbwin, S. W.; Mazzuckelli, T. J.
Tetrahedron Letters, 1986 , vol. 27, # 49 p. 5975 - 5978
反应条件
1: sodium amide; diethyl ether / nachfolgenden Einleiten von Acetylen
2: mercury (II)-oxide; diluted sulfuric acid
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参考文献
Leers
Bulletin de la Societe Chimique de France, 1926 , vol. <4>39, p. 423
参考文献
Leers
Bulletin de la Societe Chimique de France, 1926 , vol. <4>39, p. 423
反应条件
ammonia; ammonium chloride; calcium chloride
T=90 - 120°C; P=12928.7 - 18100.2 Torr; 6 h;
参考文献
Gaines,J.R.; Hansen,G.R.
Journal of Heterocyclic Chemistry, 1964 , vol. 1, p. 96 - 97