1-氨基-4-甲基环己烷合成路线 (共 20 条)
反应条件
lithium; ethylenediamine in propylamine; tert-butyl alcohol
参考文献
Allergan
Patent: US5675038 A1, 1997 ;
反应条件
hydrogen; 5 ruthenium/lithium aluminate in tetrahydrofuran T=180 - 190°C; P=41372.9 - 43958.7 Torr; 12 h; Product distribution / selectivity;
参考文献
EP1767520 A1, ;
Page/Page column 11 ;
反应条件
sodium in ethanol Heating;
参考文献
Garst; Dolby; Esfandiari; Fedoruk; Chamberlain; Avey
Journal of Organic Chemistry, 2000 , vol. 65, # 21 p. 7098 - 7104
参考文献
New Japan Chemical Co., Ltd.
Patent: US4914239 A1, 1990 ;
反应条件
propylamine; lithium; ethylenediamine in tert-butyl alcohol T=20 - 62°C; Reduction;
参考文献
Garst; Dolby; Esfandiari; Fedoruk; Chamberlain; Avey
Journal of Organic Chemistry, 2000 , vol. 65, # 21 p. 7098 - 7104
反应条件
formic acid; palladium on activated charcoal in methanol 70 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 33, # 49 p. 7477 - 7480
反应条件
1: 85 percent / aq. NH2OH*HCl, CH3COONa*H2O / 0.5 h / 40 °C 2: 70 percent / Na / ethanol / Heating View Scheme
参考文献
Farmaco, , vol. 52, # 2 p. 93 - 98
反应条件
calcium hydroxide powder bei der Destillation;
参考文献
Chemische Berichte, , vol. 40, p. 2066
反应条件
potassium hydroxide; nickel monoaluminide in methanol degradation under various conditions (HBr in glac. CH3CO2H) with preparation of nonmutagenic reaction mixtures of products; Product distributionMechanism;
参考文献
Journal of Pharmaceutical Sciences, , vol. 78, # 8 p. 652 - 659
反应条件
T=290 - 320°C; beim Leiten ueber ThO2;
参考文献
Chemiker-Zeitung, Chemische Apparatur, , vol. 34, p. 1202
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 153, p. 1207