3-甲氧基苯并(a)蒽-7,12-二酮合成路线 （共 13 条）
反应条件
1: TiCl3, LiAlH4 / tetrahydrofuran / 2 h / Heating
2: 83 percent / Fermy's salt, KH2PO4, H2O / benzene / 0.5 h
3: 94 percent / NaBH4, O2 / ethanol / 72 h
4: N-bromosuccinimide / dimethylsulfoxide; H2O / 30 h
View Scheme
参考文献
Lee; Harvey
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3502 - 3507
反应条件
1: 21 percent / trichloroacetic acid, chloranil / toluene / 288 h / 105 °C
2: 87 percent / O2, KOH / ethanol / 3 h
View Scheme
参考文献
Manning, Wayne B.; Wilbur, David J.
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 733 - 734
反应条件
1: 21 percent / trichloroacetic acid, chloranil / toluene / 288 h / 105 °C
2: 87 percent / O2, KOH / ethanol / 3 h
View Scheme
参考文献
Manning, Wayne B.; Wilbur, David J.
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 733 - 734
