2-丙烯酸-2-[[(丁基氨基)-羰基]氧代]乙酯合成路线 (共 4 条)
反应条件
hypophosphorous acid; 4-methoxy-phenol; toluene-4-sulfonic acid in toluene
T=70°C; 6 h; Reduced pressure;
参考文献
UCB, S.A.
Patent: WO2004/52843 A1, 2004 ;
Location in patent: Page 35 ;
反应条件
phenothiazine; 2,6-di-tert-butyl-4-methyl-phenol; titanium(IV) isopropylate; titanium tetra-n-butoxide
T=65°C; 10.5 h;
参考文献
UCB, S.A.
Patent: WO2004/52843 A1, 2004 ;
Location in patent: Page 34-35 ;
反应条件
novozyme 435
T=60°C; 24 h; Enzymatic reaction;
参考文献
BASF Aktiengesellschaft
Patent: US7164037 B2, 2007 ;
Location in patent: Page/Page column 18 ;
参考文献
Jansen, Johan F. G. A.; Dias, Aylvin A.; Dorschu, Marko; Coussens, Betty
Macromolecules, 2003 , vol. 36, # 11 p. 3861 - 3873