3-(3-氯苯基)-3-氧代丙酸甲酯合成路线 (共 4 条)
参考文献
Wahl; Rolland
Annales de Chimie (Cachan, France), 1928 , vol. <10> 10, p. 44
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1928 , vol. 186, p. 38
反应条件
potassium tert-butylate in tetrahydrofuran
T=16 - 31°C; 2.66667 h;
参考文献
Reddy, K. Raja; Erion, Mark D.; Matelich, Michael C.; Kopcho, Joseph J.
Patent: US2003/229225 A1, 2003 ;
Location in patent: Page 18 ;
反应条件
1: With potassium tert-butylate in tetrahydrofuran
T=16 - 31°C; 2.91667 h;
2: With hydrogenchloride; water in tetrahydrofuran
0.25 h;
参考文献
Reddy, K. Raja; Erion, Mark D.
Patent: US2005/182252 A1, 2005 ;
Location in patent: Page/Page column 38-39 ;
反应条件
sodium tetrahydroborate in methanol
T=10°C;
参考文献
Borowiecki, Pawel; Bretner, Maria
Tetrahedron Asymmetry, 2013 , vol. 24, # 15-16 p. 925 - 936