N-[2-(乙氧羰基氨基)苯基]氨基甲酸乙酯合成路线 (共 8 条)
反应条件
Ansaeuern der Reaktionsloesung mit wss.Salzsaeure;
参考文献
Darapsky; Gaudian
Journal fuer Praktische Chemie (Leipzig), 1937 , vol. <2> 147, p. 43,51
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 7 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 130, # 7 p. 2144 - 2145
反应条件
triethylamine in tetrahydrofuran
1 h; Reflux;
参考文献
Conconi, Maria Teresa; Marzaro, Giovanni; Urbani, Luca; Zanusso, Ilenia; Di Liddo, Rosa; Castagliuolo, Ignazio; Brun, Paola; Tonus, Francesca; Ferrarese, Alessandro; Guiotto, Adriano; Chilin, Adriana
European Journal of Medicinal Chemistry, 2013 , vol. 67, p. 373 - 383
反应条件
tin; ammonium chloride in methanol
T=25°C; 3.5 h; Sonication;
参考文献
Chandrasekhar; Narsihmulu; Jagadeshwar
Synlett, 2002 , # 5 p. 771 - 772
反应条件
triethylamine in benzene
3 h; Heating;
参考文献
Abe, Noritaka; Ishikawa, Naomi; Hayashi, Takashi; Miura, Yoshiaki
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 6 p. 1617 - 1622
反应条件
1: 69 percent / ethanol / 3 h / Heating
2: 29 percent / Et3N / benzene / 3 h / Heating
View Scheme
参考文献
Abe, Noritaka; Ishikawa, Naomi; Hayashi, Takashi; Miura, Yoshiaki
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 6 p. 1617 - 1622
参考文献
Darapsky; Gaudian
Journal fuer Praktische Chemie (Leipzig), 1937 , vol. <2> 147, p. 43,51
反应条件
1: acetic acid; nitric acid / 1 h / |Reflux
2: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C
3: SnCl2·2H2O / ethanol / 6 h / |Reflux
View Scheme
参考文献
Conconi, Maria Teresa; Marzaro, Giovanni; Urbani, Luca; Zanusso, Ilenia; Di Liddo, Rosa; Castagliuolo, Ignazio; Brun, Paola; Tonus, Francesca; Ferrarese, Alessandro; Guiotto, Adriano; Chilin, Adriana
European Journal of Medicinal Chemistry, 2013 , vol. 67, p. 373 - 383