双(羧甲基)三硫代碳酸盐合成路线 (共 76 条)
反应条件
potassium carbonate in water
12 h; Reflux;
参考文献
Kamila, Sukanta; Ankati, Haribabu; Harry, Emily; Biehl, Edward R.
Tetrahedron Letters, 2012 , vol. 53, # 17 p. 2195 - 2198
参考文献
Holmberg
Journal fuer Praktische Chemie (Leipzig), 1910 , vol. <2> 81, p. 456
反应条件
in water
T=95 - 100°C; 19 h;
参考文献
He, Xiao-Yang; Zou, Peng; Qiu, Jiayin; Hou, Ling; Jiang, Shibo; Liu, Shuwen; Xie, Lan
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 22 p. 6726 - 6734
反应条件
potassium carbonate in water
参考文献
Cell Therapeutics, Inc.
Patent: US2004/2526 A1, 2004 ;
反应条件
aq.-ethanolic solution of pH 8.5
参考文献
D'Angeli
Annali di Chimica (Rome, Italy), 1956 , vol. 46, p. 396,399, 402
反应条件
T=100°C; in Loesung vom pH 3.6 bis pH 14 bei unterschiedlichem Mengenverhaeltnis der Reaktionspartner und unterschiedlicher Reaktionsdauer;
参考文献
D'Angeli
Annali di Chimica (Rome, Italy), 1956 , vol. 46, p. 396,399, 402
反应条件
1: bis(carboxymethyl) trithiocarbonate With 1,1'-carbonyldiimidazole in tetrahydrofuran
T=20°C; 1.5 h;
2: cyclohexylamine in tetrahydrofuran
4 h; Reflux;
参考文献
Harada, Koichiro; Kubo, Hideki; Abe, Jun; Haneta, Mari; Conception, Arnel; Inoue, Shinichi; Okada, Satoshi; Nishioka, Kazuhiko
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 10 p. 3242 - 3254
反应条件
in water
T=95 - 100°C;
参考文献
Liu, Kun; Lu, Hong; Hou, Ling; Qi, Zhi; Teixeira, Catia; Barbault, Florent; Fan, Bo-Tao; Liu, Shuwen; Jiang, Shibo; Xie, Lan
Journal of Medicinal Chemistry, 2008 , vol. 51, # 24 p. 7843 - 7854
反应条件
potassium carbonate in water
参考文献
Cell Therapeutics, Inc.
Patent: US2004/2526 A1, 2004 ;
参考文献
Radi, Marco; Botta, Lorenzo; Casaluce, Gianni; Bernardini, Martina; Botta, Maurizio
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 1 p. 200 - 205