1,4-二溴-2,5-二碘苯合成路线 （共 27 条）
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=20°C; 10 h;
参考文献
Mouri, Kazuhiro; Wakamiya, Atsushi; Yamada, Hiroshi; Kajiwara, Takashi; Yamaguchi, Shigehiro
Organic Letters, 2007 , vol. 9, # 1 p. 93 - 96
反应条件
iodide
1.) THF, RT, 2 h, 2) THF, 10 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hart, Harold; Harada, Katsumasa; Du, Chi-Jen Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3104 - 3110
反应条件
iodine
1.) THF, room temperature; Yield given. Multistep reaction;
参考文献
Hart, Harold; Harada, Katsumasa
Tetrahedron Letters, 1985 , vol. 26, # 1 p. 29 - 32
反应条件
in tetrahydrofuran
2.5 h; Ambient temperature; Yield given;
参考文献
Hart, Harold; Harada, Katsumasa; Du, Chi-Jen Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3104 - 3110
反应条件
in tetrahydrofuran
2.5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hart, Harold; Harada, Katsumasa; Du, Chi-Jen Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3104 - 3110
反应条件
in tetrahydrofuran
2 h; Ambient temperature; Yield given;
参考文献
Hart, Harold; Harada, Katsumasa; Du, Chi-Jen Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3104 - 3110
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in toluene
T=20°C; 12 h;
参考文献
Yamaguchi, Shigehiro; Xu, Caihong; Tamao, Kohei
Journal of the American Chemical Society, 2003 , vol. 125, # 45 p. 13662 - 13663
