N2-异丁酰-2'-甲氧基鸟苷合成路线 （共 2 条）
反应条件
pyridine T=0 - 20°C; 18 h; Yield given;
参考文献
Dimock, Stuart; Bhat, Balkrishen; Peoc'h, Didier; Sanghvi, Yogesh S.; Swayze, Eric E.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1629 - 1632
反应条件
Multi-step reaction with 7 steps 1.1: pyridine; DMAP / 20 °C2.1: 3.5 g / DMAP; Et3N / CH2Cl2 / 2 h / 20 °C3.1: DABCO / dioxane / 0.5 h / 20 °C3.2: DBU / dioxane / 20 °C4.1: 1.1 g / aq. NaOH / tetrahydrofuran; methanol / 0.08 h / 0 °C5.1: 70 percent / NaH / dimethylformamide / 1.5 h / 0 °C6.1: pyridine / 1 h / 20 °C7.1: 90 percent / TBAF / tetrahydrofuran / 1 h / 20 °C
参考文献
Zlatev, Ivan; Vasseur, Jean-Jacques; Morvan, Francois Tetrahedron, 2007 , vol. 63, # 45 p. 11174 - 11178
