3-丙基环己-2-烯-1-酮合成路线 （共 12 条）
反应条件
hydrogenchloride in tetrahydrofuran
T=50°C; 4 h;
参考文献
Yoshida, Takashi; Saito, Shojiro
Chemistry Letters, 1982 , p. 165 - 168
反应条件
hydroxocobalamine hydrochloride; lithium perchlorate; NH4Br in N,N-dimethyl-formamide
T=20°C; electrolysis;
参考文献
Scheffold, Rolf; Dike, Meera; Dike, Sunneel; Herold, Thomas; Walder, Lorenz
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3642 - 3644
反应条件
1: in diethyl ether
T=0 - 20°C; Inert atmosphere;
2: With hydrogenchloride in water
T=20°C; Inert atmosphere;
参考文献
Shintani, Ryo; Takeda, Momotaro; Nishimura, Takahiro; Hayashi, Tamio
Angewandte Chemie - International Edition, 2010 , vol. 49, # 23 p. 3969 - 3971
反应条件
in tetrahydrofuran
T=0 - 25°C;
参考文献
MERCK and CO., INC.
Patent: WO2007/75749 A2, 2007 ;
Location in patent: Page/Page column 54 ;
反应条件
copper(l) iodide in diethyl ether
T=0°C; 1 h;
参考文献
Majetich, George; Defauw, Jean; Ringold, Clay
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 50 - 68
反应条件
in diethyl ether
T=0°C; 2 h;
参考文献
Majetich, George; Defauw, Jean; Ringold, Clay
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 50 - 68
反应条件
1: in diethyl ether
T=20°C; 0.5 h;
2: With sulfuric acid in diethyl ether; water
参考文献
Kyte, Brian G.; Rouviere, Pierre; Cheng, Qiong; Stewart, Jon D.
Journal of Organic Chemistry, 2004 , vol. 69, # 1 p. 12 - 17
反应条件
1: LDA
2: 90 percent / 5 percent hydrochloric acid / tetrahydrofuran / 4 h / 50 °C
View Scheme
参考文献
Yoshida, Takashi; Saito, Shojiro
Chemistry Letters, 1982 , p. 165 - 168
反应条件
Ni(salen); 2,3,5-trimethylfurolt;2,3-egt;pyranolt;2,3-bgt;pyridin-7-one in N,N-dimethyl-formamide
electrochemical reduction; Product distribution;
参考文献
Mubarak, Mohammad S.; Pagel, Marty; Marcus, Lawrence M.; Peters, Dennis G.
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 1319 - 1322
参考文献
Ferard-Brunner,J. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1972 , vol. 274, p. 2111 - 2114
