1-(3,4-亚甲二氧基苯基)乙醇合成路线 （共 17 条）
反应条件
N-bromosuccinmide in acetonitrile
T=20°C; 0.5 h;
参考文献
Joncour, Agnes; Decor, Anne; Liu, Jian-Miao; Tran Huu Dau, Marie-Elise; Baudoin, Olivier
Chemistry - A European Journal, 2007 , vol. 13, # 19 p. 5450 - 5465
反应条件
durch Destillation unter vermindertem Druck;
参考文献
Schmidt; Kircher; Kunz; Wahl; Hendriok
Journal of Organic Chemistry, 1995 , vol. 60, # 12 p. 3890 - 3894
反应条件
1: 8.99 g / CrO3/conc. H2SO4 / H2O; acetone / 1 h / 10 °C
2: 0.68 g / 10percent aq. NaOH / ethanol / Ambient temperature
3: 11.0 g / 2-ethoxy-ethanol; acetic acid; H2O / 0.25 h / 120 °C
View Scheme
参考文献
Ishii; Ishikawa; Deushi; et al.
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 9 p. 3024 - 3038
反应条件
1: 8.99 g / CrO3/conc. H2SO4 / H2O; acetone / 1 h / 10 °C
2: 122.2 g / 10percent aq. NaOH / ethanol / Ambient temperature
View Scheme
参考文献
Ishii, Hisashi; Ishikawa, Tsutomu; Chen, Ih-Sheng; Ichikawa, Yuh-Ichiro
Heterocycles, 1984 , vol. 21, # 2 p. 711
反应条件
1: 8.99 g / CrO3/conc. H2SO4 / H2O; acetone / 1 h / 10 °C
2: 27.9 g / 10percent aq. NaOH / ethanol / Ambient temperature
View Scheme
参考文献
Ishii; Ishikawa; Deushi; et al.
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 9 p. 3024 - 3038
反应条件
iodine; silver trifluoroacetate in chloroform
T=0°C; 0.25 h;
参考文献
Joncour, Agnes; Decor, Anne; Liu, Jian-Miao; Tran Huu Dau, Marie-Elise; Baudoin, Olivier
Chemistry - A European Journal, 2007 , vol. 13, # 19 p. 5450 - 5465
反应条件
1: Jones reagent
2: OH-
3: acetic acid / 2-ethoxy-ethanol
View Scheme
参考文献
Ishii; Ishikawa; Deushi; et al.
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 9 p. 3024 - 3038
