反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iodine; hexacarbonyl chromium
1.) dibutyl ether, THF, 24 h, reflux, 2.) THF, -78 deg C, 1 h, 3.) THF, -78 deg C, 20 min, 4.) THF, 0 deg C, 40 h, 5.) THF, -78 deg C, 2 min, 6.) THF, 20 h, room temp.; Yield given. Multistep reaction;
参考文献
Cambie, Richard C.; Clark, George R.; Gallagher, Stewart R.; Rutledge, Peter S.; Stone, Martin J.; Woodgate, Paul D.
Journal of Organometallic Chemistry, 1988 , vol. 342, p. 315 - 338
