(4-烯丙基-2-甲氧基苯氧基)乙酸合成路线 (共 7 条)
反应条件
1: potash; amyl alcohol / 145 °C 2: sulfuric acid; potassium dichromate / Behandeln des dadurch erhaltenen 2-Methoxy-4-formyl-phenoxessigsaeures mit PCl5 bei 130grad und Zersetzen des Reaktionsproduktes mit kochendem Wasser View Scheme
参考文献
Gassmann; Krafft
Chemische Berichte, 1895 , vol. 28, p. 1870
反应条件
bei der Kalischmelze;
参考文献
Lederer
Patent: DE80747 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 151
反应条件
1: With triethylamine in N,N-dimethyl-formamide; toluene Curtius rearrangement; 3 h; Heating; 2: With potassium hydroxide; glycerol in ethanol; N,N-dimethyl-formamide; toluene 2 h; Heating; Further stages.;
参考文献
Spurg, Anke; Waldvogel, Siegfried R.
European Journal of Organic Chemistry, 2008 , # 2 p. 337 - 342
反应条件
1: potash; amyl alcohol / 145 °C 2: water; KMnO4; acetic acid / Reagens 4:NaOH View Scheme
参考文献
Gassmann; Krafft
Chemische Berichte, 1895 , vol. 28, p. 1870
反应条件
sodium hydroxide
T=20 - 50°C; Substitution; 8 h;
参考文献
Labarrios, Fernando; Garduno, Leticia; Vidal, Maria Del Rosario; Garcia, Raul; Salazar, Maria; Martinez, Elizdath; Diaz, Francisco; Chamorro, German; Tamariz, Joaquin
Journal of Pharmacy and Pharmacology, 1999 , vol. 51, # 1 p. 1 - 7
反应条件
sodium hydride in tetrahydrofuran
12 h; Heating;
参考文献
Abraham, D. J.; Kennedy, P. E.; Mehanna, A. S.; Patwa, D. C.; Williams, F. L.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 8 p. 967 - 978
参考文献
Varma, R. Luxmi; Narayanan, C. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 302 - 304