6-甲氧基-1a,2,3,7b-四氢-1-噁-环丙[a]萘合成路线 （共 5 条）
反应条件
zinc(II) iodide in benzene 3 h; Heating;
参考文献
Okumura, Kunio; Shimazaki, Toshiyuki; Aoki, Yoji; Yamashita, Hiroyuki; Tanaka, Eishi; Banba, Shinichi; Yazawa, Kouhei; Kibayashi, Kenji; Banno, Hitoshi
Journal of Medicinal Chemistry, 1998 , vol. 41, # 21 p. 4036 - 4052
反应条件
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid in toluene
2 h; Ambient temperature;
参考文献
Okumura, Kunio; Shimazaki, Toshiyuki; Aoki, Yoji; Yamashita, Hiroyuki; Tanaka, Eishi; Banba, Shinichi; Yazawa, Kouhei; Kibayashi, Kenji; Banno, Hitoshi
Journal of Medicinal Chemistry, 1998 , vol. 41, # 21 p. 4036 - 4052
反应条件
sodium hydride in tetrahydrofuran
T=20°C; 4 h;
参考文献
Peglion, Jean-Louis; Dessinges, Aimee; Goument, Bertrand; Millan, Mark; La Cour, Clotilde Mannoury
Patent: US2006/229318 A1, 2006 ;
Location in patent: Page/Page column 10 ;
US 20060229318 A1
反应条件
1: 51.1 g / NaBH4 / methanol; tetrahydrofuran / 2 h / Ambient temperature
2: pyridinium p-toluenesulfonate / toluene / 3 h / Heating
3: 95 percent / 10percent aq. NaHCO3, 3-chloroperbenzoic acid / toluene / 2 h / Ambient temperature
View Scheme
参考文献
Okumura, Kunio; Shimazaki, Toshiyuki; Aoki, Yoji; Yamashita, Hiroyuki; Tanaka, Eishi; Banba, Shinichi; Yazawa, Kouhei; Kibayashi, Kenji; Banno, Hitoshi
Journal of Medicinal Chemistry, 1998 , vol. 41, # 21 p. 4036 - 4052
反应条件
1: pyridinium p-toluenesulfonate / toluene / 3 h / Heating
2: 95 percent / 10percent aq. NaHCO3, 3-chloroperbenzoic acid / toluene / 2 h / Ambient temperature
View Scheme
参考文献
Okumura, Kunio; Shimazaki, Toshiyuki; Aoki, Yoji; Yamashita, Hiroyuki; Tanaka, Eishi; Banba, Shinichi; Yazawa, Kouhei; Kibayashi, Kenji; Banno, Hitoshi
Journal of Medicinal Chemistry, 1998 , vol. 41, # 21 p. 4036 - 4052
