(2-羟基-1-萘基)苯基甲酮合成路线 (共 35 条)
反应条件
aluminium trichloride; tetrachloroethane, 1,1,2,2-
参考文献
Fieser
Journal of the American Chemical Society, 1931 , vol. 53, p. 3546,3555
反应条件
boron trifluoride diethyl etherate in benzene
crossover Friess rearrangement; 3 h; Heating;
参考文献
Khanna, R. N.; Singh, K. P.; Sharma, Jyotsana
Organic Preparations and Procedures International, 1992 , vol. 24, # 6 p. 687 - 690
反应条件
boron trifluoride diethyl etherate in benzene
cross Fries reaction; 0.5 h; microwave irradiation;
参考文献
Thapliyal; Aggarwal
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 9 p. 706 - 708
反应条件
iron(III) chloride on silica
T=70 - 72°C;
参考文献
Bendale, Pravin M.; Khadilkar, Bhushan M.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 8 p. 1738 - 1739
反应条件
1: ethanol / 12 h / 20 °C / |Reflux
2: copper (II) acetate monohydrate; diacetoxymethylbenzene / cis-1,2-dichloroethylene / 3 h / 90 °C / |Green chemistry
View Scheme
参考文献
Deb, Mohit L.; Dey, Suvendu S.; Bento, Isabel; Barros, M. Teresa; Maycock, Christopher D.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9791 - 9795
Angew. Chem., 2013 , vol. 125, # 37 p. 9973 - 9977,5
反应条件
1: ethanol / 12 h / 20 °C / |Reflux
2: copper (II) acetate monohydrate; diacetoxymethylbenzene / cis-1,2-dichloroethylene / 3 h / 90 °C / |Green chemistry
View Scheme
参考文献
Deb, Mohit L.; Dey, Suvendu S.; Bento, Isabel; Barros, M. Teresa; Maycock, Christopher D.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9791 - 9795
Angew. Chem., 2013 , vol. 125, # 37 p. 9973 - 9977,5
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride
T=60°C; Zersetzen des Reaktionsprodukts mit Eis;
参考文献
Houben; Fischer
Chemische Berichte, 1927 , vol. 60, p. 1768
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 123, p. 273
参考文献
Phadke; Shah
Journal of the Indian Chemical Society, 1950 , vol. 27, p. 349,353
反应条件
1,4-dioxane; sulfuric acid
Hydrolysis;
参考文献
Chauvellier
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1951 , vol. 232, p. 2458
反应条件
2: dioxane; aqueous H2SO4 / Hydrolysis
View Scheme
参考文献
Chauvellier
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1951 , vol. 232, p. 2458