2-亚甲基-1-邻苯二甲酰亚胺基丙烷合成路线 （共 8 条）
反应条件
jones reagent; osmium(VIII) oxide in water; acetone 20 h; Ambient temperature;
参考文献
Henry, James R.; Weinreb, Steven M.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4745
反应条件
Aliquatreg; 336 in N,N-dimethyl-formamide
T=20°C;
参考文献
Schmidt, Axel M.; Eilbracht, Peter
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 12 p. 2333 - 2343
反应条件
in DMF (N,N-dimethyl-formamide)
T=90°C; 4 h;
参考文献
LA JOLLA PHARMACEUTICAL COMPANY
Patent: WO2005/82343 A2, 2005 ;
Location in patent: Page/Page column 80 ;
反应条件
Aliquatreg; 336; potassium carbonate in N,N-dimethyl-formamide
20 h;
参考文献
Koc, Fikret; Eilbracht, Peter
Tetrahedron, 2004 , vol. 60, # 38 p. 8465 - 8476
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene
T=110°C; P=760.051 Torr; 24 h; Ionic liquidAutoclave;
参考文献
Cao, Hong; Alper, Howard
Organic Letters, 2010 , vol. 12, # 18 p. 4126 - 4129
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran
T=90°C; 7 h; Inert atmosphere; chemoselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Green Chemistry, 2010 , vol. 12, # 8 p. 1380 - 1382
反应条件
in acetic acid
0.5 h; Heating;
参考文献
Stille, J. K.; Becker Y.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2139 - 2145
反应条件
triphenylphosphine; diethylazodicarboxylate
T=0 - 20°C; 18 h; Inert atmosphereSchlenk technique;
参考文献
Zheng, Xin; Cao, Bonan; Liu, Tang-Lin; Zhang, Xumu
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 679 - 684
