in hexane boronic acid was treated with an equiv. amt. of Me2C(OH)CMe2(OH)*H2O inhexane overnight; distilled from a little galvinoxyl to prevent polymerization; elem. anal.;
参考文献
Matteson, Donald S.; Majumdar, Debesh
Organometallics, 1983 , vol. 2, p. 230 - 236
in benzene byproducts: H2O; under Ar, soln. of allylboronic acid in C6H6 treated with 2-propanol (2 equiv), heated to reflux until evolution of H2O completed (Dean-Stark trap); fractionally distd. (bp 62-64°C, 40 mmHg);
参考文献
Roush, William R.; Walts, Alan E.; Hoong, Lee K.
Journal of the American Chemical Society, 1985 , vol. 107, # 26 p. 8186 - 8190
in benzene byproducts: H2O; under Ar, soln. of allylboronic acid in C6H6 treated with 2-propanol (2 equiv), heated to reflux until evolution of H2O completed (Dean-Stark trap); fractionally distd. (bp 62-64°C, 40 mmHg);
参考文献
Roush, William R.; Walts, Alan E.; Hoong, Lee K.
Journal of the American Chemical Society, 1985 , vol. 107, # 26 p. 8186 - 8190
