N-(4-羟基-2,6-二甲基苯基)乙酰胺合成路线 （共 9 条）
反应条件
sodium dithionite; water in ethyl acetate T=50°C; 0.0833333 h;
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
sodium acetate in water 1 h;
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
1: 1.) diazotized sulfanilic acid, 2.) sodium dithionite / 1.) 1 h, 2.) 65 deg C to 70 deg C 2: 89 percent / NaOAc / H2O / 1 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 23, # 11 p. 1153 - 1158
反应条件
sodium carbonate in diethyl ether; water T=0°C; 0.416667 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 4 p. 653 - 662
反应条件
1: acetonitrile / 1.17 h / Heating 2: H2O, phosphate buffer / acetonitrile / 0.33 h / 40 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 4 p. 653 - 662
参考文献
DE291499 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 13, p. 501
反应条件
acetate buffer; sodium perchlorate; sodium bromide in acetonitrile T=40°C; var. conc. of NaBr, also without NaBr, other O-aroyl-N-(2,6-dimethylphenyl)hydroxylamines; var. pH; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 4 p. 663 - 672
反应条件
1: 41 percent / Pb(OAc)4 / ethyl acetate / 45 °C 2: 76 percent / H2O / acetone / 6 h / Heating View Scheme
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
lead(IV) acetate in ethyl acetate
T=45°C;
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
