N-(4-甲基-3-硝基苯基)氨基甲酸甲酯合成路线 (共 3 条)
反应条件
tetraethylammonium chloride; tri-ruthenium(0)dodecacarbonyl in toluene
T=160 - 170°C; P=82 Torr; 5 h;
参考文献
Cenini, Sergio; Pizzotti, Maddalena; Crotti, Corrado; Porta, Francesca; Monica, Girolamo La
Journal of the Chemical Society, Chemical Communications, 1984 , # 19 p. 1286 - 1287
反应条件
1: methyl chloroformate With zinc in toluene
T=20°C; 0.166667 h;
2: 1-amino-3-nitro-4-methylbenzene in toluene
T=20°C; 72 h;
参考文献
Gasperini, Michela; Ragaini, Fabio; Cazzaniga, Chiara; Cenini, Sergio
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 1 p. 105 - 120
反应条件
phenyl-phosphonic acid; 2,2-dimethoxy-propane; 2-Methyl-5-nitro-phenylamine; {Pd([1,10]phenanthroline)2}[BF4]2
T=150°C; P=45003.6 Torr; 5 h; Product distributionKinetics; Further Variations:ReagentsTemperaturesPressuresCatalysts;
参考文献
Gasperini, Michela; Ragaini, Fabio; Cazzaniga, Chiara; Cenini, Sergio
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 1 p. 105 - 120