5-羟甲基-2-呋喃甲酸合成路线 （共 46 条）
反应条件
citrate buffer; dihydrogen peroxide; chloroperoxidase (E.C. 1.11.1.10) in water T=20°C; Oxidation; pH=5; 2.5 h;
参考文献
Van Deurzen; Van Rantwijk; Sheldon
Journal of Carbohydrate Chemistry, 1997 , vol. 16, # 3 p. 299 - 309
反应条件
nitric acid T=100°C; 22 h;
参考文献
Polish Journal of Chemistry, , vol. 68, # 4 p. 693 - 698
反应条件
1: hydrogen chloride 2: tetrachloromethane; hydrogen chloride View Scheme
参考文献
Haworth; Jones
Journal of the Chemical Society, 1944 , p. 667,670
反应条件
1: 53 percent / conc. H2SO4 / 3 h / Heating
2: 63 percent / ZnCl2 / CHCl3 / 1 h / 20 °C
3: 75 percent / acetic acid / 6 h / Heating
4: 80 percent / 51percent HNO3 / 1.) reflux, 2.) room. temp., 24 h
5: 78 percent / SOCl2, pyridine / benzene / 6 h / Heating
View Scheme
参考文献
Nielek, S.; Leslak, T.
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 5 p. 825 - 829
参考文献
Talaga, Patrice; Matagne, Alain; Klitgaard, Henrik
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 10 p. 1313 - 1316
反应条件
1: 53 percent / conc. H2SO4 / 3 h / Heating
2: 19 percent / ZnCl2 / CHCl3 / 1 h / 20 °C
3: 91.5 percent / 20percent NaOH / H2O / 3 h / Heating
View Scheme
参考文献
Nielek, S.; Leslak, T.
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 5 p. 825 - 829
