2-[2-(2-AMINOETHOXY)ETHOXY]ETHANOL合成路线 (共 22 条)
反应条件
1: ethanol 2: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 4 h 3: sodium hydroxide / water; toluene / 100 °C 4: triethylamine / dichloromethane 5: sodium azide / N,N-dimethyl-formamide / 70 °C 6: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Gerard, Estelle; Meulle, Aline; Feron, Olivier; Marchand-Brynaert, Jacqueline
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 586 - 590
反应条件
sodium hydrogencarbonate in water
Inert atmosphere;
参考文献
Jalisatgi, Satish S.; Kulkarni, Vikas S.; Tang, Betty; Houston, Zachary H.; Lee, Mark W.; Hawthorne, M. Frederick
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12382 - 12385