2,2,3,3,4,4,5,5,6-九溴联苯合成路线 （共 7 条）
反应条件
1: With bromine
T=40°C;
2: With bromine; AlCl3, aluminium chloride
T=56.5 - 78.4°C; P=1385.82 - 1458.22 Torr; 3.65 - 4.36667 h; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27776 A2, 2008 ;
Location in patent: Page/Page column 14-15 ;
反应条件
bromine; AlCl3, aluminium chloride
T=55 - 61°C; 6.25 h; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27776 A2, 2008 ;
Location in patent: Page/Page column 8-9 ;
反应条件
1: With bromine
T=63°C; 1.25 h;
2: With bromine; AlCl3, aluminium chloride
T=59°C; 3.93333 h; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27776 A2, 2008 ;
Location in patent: Page/Page column 9-10 ;
反应条件
in methanol; water
1.66667 h; UV-irradiation; KineticsQuantum yield; Further Variations:SolventsReagents;
参考文献
Eriksson, Johan; Green, Nicholas; Marsh, Goeran; Bergman, Ake
Environmental Science and Technology, 2004 , vol. 38, # 11 p. 3119 - 3125
反应条件
bromine; bromine chloride; AlCl3, aluminium chloride
T=56°C; 0.0666667 h; Heating / reflux; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27780 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
Pschor Arylation; Electrochemical reaction;
参考文献
Rotko, Grzegorz; Romanczyk, Piotr P.; Kurek, Stefan S.
Electrochemistry Communications, 2013 , vol. 37, p. 64 - 67
反应条件
honey in acetone
T=60°C; 672 h; Darkness;
参考文献
Wang, Jun; Kliks, Michael M.; Jun, Soojin; Li, Qing X.
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 6 p. 3495 - 3501
