1,2,3-三甲氧基苯合成路线 （共 210 条）
反应条件
lithium borohydride; C30H21F6N2NiO2P in tetrahydrofuran T=70°C; 3 h; Schlenk techniqueInert atmosphere;
参考文献
Enthaler, Stephan; Weidauer, Maik; Irran, Elisabeth; Epping, Jan Dirk; Kretschmer, Robert; Someya, Chika I.
Journal of Organometallic Chemistry, 2013 , vol. 745-746, p. 262 - 274
反应条件
hydrogen; diethylamine; palladium on activated charcoal in methanol T=20°C; 4 h;
参考文献
Mori, Akinori; Mizusaki, Tomoteru; Ikawa, Takashi; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 5 p. 1270 - 1280
反应条件
1: 1,2,3-benzenetriol With sodium hydroxide in acetone T=20°C; 0.5 h; 2: dimethyl sulfate in acetone T=20°C; 10 h;
参考文献
Jing, Xiao-Bi; Wang, Li; Han, Ying; Shi, Yao-Cheng; Liu, Yong-Hong; Sun, Jing
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 5 A p. 1001 - 1004
反应条件
palladium diacetate in cyclohexane T=140°C; 24 h; Molecular sieveair;
参考文献
Modak, Atanu; Deb, Arghya; Patra, Tuhin; Rana, Sujoy; Maity, Soham; Maiti, Debabrata
Chemical Communications, 2012 , vol. 48, # 35 p. 4253 - 4255
反应条件
bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine; trifluoroacetic acid in N,N-dimethyl-formamide T=55°C; 9 h;
参考文献
Semmelhack, M.F.; Helquist, Paul; Jones, L.D.; Keller, Leonard; Mendelson L.; et al.
Journal of the American Chemical Society, 1981 , vol. 103, # 21 p. 6460 - 6471
反应条件
ammonium formate; tri-ruthenium(0)dodecacarbonyl in 1,4-dioxane T=160°C; 20 h;
参考文献
Chatani; Tatamidani; Ie; Kakiuchi; Murai
Journal of the American Chemical Society, 2001 , vol. 123, # 20 p. 4849 - 4850
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II); 1,3-bis-(diphenylphosphino)propane; triethylamine in toluene T=100°C; 18 h; Inert atmosphere;
参考文献
Rosen, Brad M.; Huang, Chenghong; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 12 p. 2597 - 2600
反应条件
sodium acetate; magnesium; palladium on activated charcoal in methanol T=20°C; 24 h;
参考文献
Organic Letters, , vol. 8, # 5 p. 987 - 990
反应条件
potassium hydroxide; Sec-butyl alcohol; palladium diacetate; triphenylphosphine T=100°C; 1 h;
参考文献
Chen, Jingbo; Zhang, Yushun; Yang, Liquan; Zhang, Xiang; Liu, Jianping; Li, Liang; Zhang, Hongbin
Tetrahedron, 2007 , vol. 63, # 20 p. 4266 - 4270
反应条件
1: aq. K3PO4 / toluene / 0.5 h 2: Mg; methanol / Pd/C / 12 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1432 - 1441
