1,2,3-三甲氧基苯合成路线 （共 210 条）
参考文献
Marini-Bettolo; Ballio; Baroni
Gazzetta Chimica Italiana, 1948 , vol. 78, p. 301
参考文献
Harding
Journal of the Chemical Society, 1914 , vol. 105, p. 2794
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in various solvent(s) 0.25 h; Ambient temperature;
参考文献
Kita, Yasuyuki; Tohma, Hirofumi; Hatanaka, Kenji; Takada, Takeshi; Fujita, Shigekazu; Mitoh, Shizue; Sakurai, Hiromu; Oka, Shigenori
Journal of the American Chemical Society, 1994 , vol. 116, # 9 p. 3684 - 3691
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 17 h; Reagent/catalyst; Overall yield = 38 percent; Overall yield = 97.4 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
反应条件
palladium diacetate in acetic anhydride; acetic acid T=100°C; Overall yield = 26 percentChromat.;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
反应条件
1: NaBr; acetic acid; H2O2 / H2O / 2 h / 20 °C 2: 18 g / CuCl / dimethylformamide / 9 h / 110 °C View Scheme
参考文献
Asakawa, Tomohiro; Hiza, Aiki; Nakayama, Miho; Inai, Makoto; Oyama, Dai; Koide, Hiroyuki; Shimizu, Kosuke; Wakimoto, Toshiyuki; Harada, Norihiro; Tsukada, Hideo; Oku, Naoto; Kan, Toshiyuki
Chemical Communications, 2011 , vol. 47, # 10 p. 2868 - 2870
反应条件
1) K 1) THF, RT, 24h, 2) THF, -30 deg C, 3h; Yield given. Multistep reaction;
参考文献
Azzena, Ugo; Denurra, Teresa; Melloni, Giovanni; Piroddi, Anna Maria
Journal of Organic Chemistry, 1990 , vol. 55, # 19 p. 5386 - 5390
反应条件
acetic acid in tetrahydrofuran; N-methyl-acetamide; hexane
参考文献
Tanabe Seiyaku Co., Ltd.
Patent: US5849732 A1, 1998 ;
反应条件
titanium tetrachloride in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Asakawa, Tomohiro; Hiza, Aiki; Nakayama, Miho; Inai, Makoto; Oyama, Dai; Koide, Hiroyuki; Shimizu, Kosuke; Wakimoto, Toshiyuki; Harada, Norihiro; Tsukada, Hideo; Oku, Naoto; Kan, Toshiyuki
Chemical Communications, 2011 , vol. 47, # 10 p. 2868 - 2870
参考文献
Buu-Hoi et al.
Journal of Organic Chemistry, 1954 , vol. 19, p. 1548,1549
Full Text Show Details
Sapewalowa; Koton
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2900,2902; engl. Ausg. S. 2860, 2862
Full Text Show Details
Gutsche; Jason
Journal of the American Chemical Society, 1956 , vol. 78, p. 1184,1186
