1,2,3-三甲氧基苯合成路线 （共 210 条）
反应条件
[Ir(μ-Cl)(cyclooctene)2]2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; lithium chloride in water; 1,3,5-trimethyl-benzene T=170°C; 20 h; Schlenk techniqueInert atmosphere;
参考文献
Olsen, Esben P. K.; Madsen, Robert
Chemistry - A European Journal, 2012 , vol. 18, # 50 p. 16023 - 16029
反应条件
potassium carbonate in acetone
参考文献
Xia; Wang, Wei
Monatshefte fur Chemie, 2011 , vol. 142, # 1 p. 93 - 96
反应条件
hydrogenchloride; sodium hydroxide in water
反应条件
1: With magnesium in tetrahydrofuran T=20°C; 3 h; Inert atmosphere; 2: With synthetic air; cobalt(II) chloride in tetrahydrofuran T=0°C; 0.5 h; Inert atmosphere;
参考文献
Synlett, , # 18 p. 2919 - 2923
反应条件
oxygen; copper diacetate; silver carbonate in N,N-dimethyl-formamide T=145°C; 18 h;
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9938 - 9941
反应条件
Pd-PEPPSI-IPent; potassium hydroxide in tetrahydrofuran T=70°C; Suzuki-Miyaura Coupling; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 42 p. 17470 - 17473
反应条件
1: With tert.-butyl lithium in tetrahydrofuran T=-80°C; 0.166667 h; Schlenk techniqueInert atmosphere; 2: With methanol in tetrahydrofuran T=-75°C; Inert atmosphereSchlenk technique;
参考文献
Organic Letters, , vol. 15, # 12 p. 2954 - 2957
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=90°C; 5 h; Product distribution; Further Variations:TemperaturesSolventsPressuresreaction times; microwave irradiation;
参考文献
Shieh, Wen-Chung; Dell, Steven; Repic, Oljan
Organic Letters, 2001 , vol. 3, # 26 p. 4279 - 4281
反应条件
sodium hydroxide; boric acid T=20 - 25°C; 2 h; pH 10.0 - 10.4;
参考文献
Shirasaka, Tadashi; Takuma, Yuki; Imaki, Naoshi
Synthetic Communications, 1990 , vol. 20, # 8 p. 1213 - 1221
反应条件
air; sodium carbonate; palladium diacetate in ethanol 72 h; Ambient temperature;
参考文献
Synlett, , vol. 1997, # 1 p. 131 - 132
