1-(2-溴-5-甲氧基苯基)乙酮合成路线 （共 13 条）
反应条件
silica gel; pyridinium chlorochromate in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Mahendar, Lodi; Krishna, Jonnada; Gopi Krishna Reddy, Alavala; Venkat Ramulu, Bokka; Satyanarayana, Gedu
Organic Letters, 2012 , vol. 14, # 2 p. 628 - 631
反应条件
in toluene T=0 - 20°C; 0.5 h;
参考文献
Genelabs Technologies, Inc.
Patent: US2007/32488 A1, 2007 ;
Location in patent: Page/Page column 28-29 ;
反应条件
N-bromosuccinmide; sulfuric acid in water T=60°C; 5 h;
参考文献
Pravst, Igor; Zupan, Marko; Stavber, Stojan
Tetrahedron Letters, 2006 , vol. 47, # 27 p. 4707 - 4710
反应条件
1: Jones reagent View Scheme
参考文献
Australian Journal of Chemistry, , vol. 59, # 7 p. 445 - 456
反应条件
in tetrahydrofuran; diethyl ether T=0 - 20°C; Inert atmosphere;
参考文献
Thome, Isabelle; Besson, Claire; Kleine, Tillmann; Bolm, Carsten
Angewandte Chemie - International Edition, 2013 , vol. 52, # 29 p. 7509 - 7513
Angew. Chem., 2013 , vol. 125, # 29 p. 7657 - 7661,5
反应条件
1: 98 percent / SOCl2 / 18 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 120, p. 1151 - 1174
反应条件
1: 95 percent / Br2 / acetic acid 2: 98 percent / SOCl2 / 18 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 120, p. 1151 - 1174
反应条件
1: 31 percent / KMnO4 2: 95 percent / Br2 / acetic acid 3: 98 percent / SOCl2 / 18 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 120, p. 1151 - 1174
反应条件
1: bromine 2: Jones reagent View Scheme
参考文献
Australian Journal of Chemistry, , vol. 59, # 7 p. 445 - 456
反应条件
n-butyllithium; sulfuric acid Yield given. Multistep reaction;
参考文献
Journal of Chemical Research, Miniprint, , # 2 p. 526 - 541
